HowdoesUCIrunOChemlabs.pptVIP

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HowdoesUCIrunOChemlabs.ppt

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HowdoesUCIrunOChemlabs

How does UCI run O-Chem labs J. K. Kim ENROLLMENT STATISTICS 51LA WINTER 2007 SCHEDULE OF EXPERIMENTS EXP #1 - Monday, January 8 - Friday, January 12, 2007 Recrystallization of Salicylic Acid and Bromoacetanilide Read “Techniques..” pp. 100-105 (9.1-9.4), 111 (9.7a), 114 (9.8)-116 (9.9) Supplementary information in Paula Y. Bruice (4th ed): Chapters 1 2. EXP #2 - Tuesday, January 16 - Monday, January 22, 2007 Identification of a White Solid. Supplementary information in Paula Y. Bruice (4rd ed): Chapters 1 2. Read “Techniques..”10, pp. 116-126 and “Modern Projects..” pp. 239-241 EXP #3 - Tuesday, January 23 - Monday, January 29, 2007 Extraction, Drying Agents, and Sublimation. Read “Tech..” Read “Techniques..”, 8.1-8.3 (pp. 75-84), 8.5-8.10 (pp. 85-98), and 12.1-12.2 (pp. 158-160) Supplementary information in Paula Y. Bruice (4rd ed): Chapters 1 2. Exp. 1: Extraction of Caffeine from Tea. Microscale Procedure, pp. 6-8 in “Modern Projects..”. Exp. 2. Purification and Thin Layer Chromatographic Analysis of Caffeine. Microscale Procedure, pp. 9-14 in “Modern Projects..”. Do the purification by sublimation part only. EXP #4 - Tuesday, January 30 - Monday, February 5, 2007 Thin Layer Chromatography. Read “Tech..” 15.1-15.8 (pp. 177-189) Thin-Layer Chromatography. Handout Experiment #4. EXP #5 –Tuesday, February 6 - Monday, February 12, 2007 Separation of Organic Mixtures Read “Techniques..” 8, pp. 75-99) Supplementary information in Paula Y. Bruice (4rd ed), Chapters 1 2 Project 2. Using Extraction to Separate a Mixture, pp. 243-246 in “Modern Projects..” 2.1 Separation and Purification of the Compounds in the Unknown Mixture: First Week. Miniscale Procedure, 245 in “Modern Projects..” 2.2 Melting Points, purity, and Identification of the Compounds in the Mixture: Second Week. Miniscale Procedure, 246 in “Modern Projects..” (Extra Credit) EXP #6 - Tuesday, February 13 - Wednesday, February 21, 2007 Boiling Points and Distillation NOTE: Students i