Formation of Monolayer Films by the Spontaneous Assembly of Organic Thiols from Solution onto Gold.pdf

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Formation of Monolayer Films by the Spontaneous Assembly of Organic Thiols from Solution onto Gold.pdf

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Formation of Monolayer Films by the Spontaneous Assembly of Organic Thiols from Solution onto Gold

J. Am. Chem. SOC. 1989, 1 1 1 , 321-335 321 (q, 1 H, J = 6.7 Hz); MS, m / e 93 (58), 107 (loo), 149 (51), 166 (33), 209 (29), 224 (15); exact mass calcd for CI4H24O2 224.178 26, found 224.178 20. Registry No. 5, 19945-61-0; 7, 19954-66-6; 8, 110990-63-1; 9, 280-64-8; B-CH,(CH2),-9-BBN, 30089-00-0; B-Me-9-BBN, 2341 8-8 1-7; CH3(CH2)7B(Sia)2, 32327-50-7; CH3(CH2)7B(c-C,H,,)2, 38103-67-2; 38388-16-8; 11, 117582-51-1; 15, 117582-60-2; 16, 117582-59-9; 9-BBN, 7 PdCl,(dppf), 72287-26-4; Pd(PPh3)4, 14221-01-3; CH,(CH,)?BOCH2- . .. - CH2CH20, 117582-36-2; s-Bu~B, 1 1 13-78-6; Pd(OAc),, 3375-31-3; PdCI,. 7647-10-1: o-MeOC6Hal, 529-28-2; CH2=CH(CH2)N, I 53179-04-7; CHZ=CH(CH2)2C(CH3)OCH2, 1 17582-37-3; CH2=CH- ~~ (CH2),C(CH,)OCH2CH20, 20449-2 1-2; (E)-PhCH=CHBr, 588-72-7; PhCH=CH’. 23065-05-6; (Z)-PhCH=CHBr, 588-73-8; (CH,),C=C- HBr, 301 7-69-4; (Z)-CH3CH=CBrCH3, 3017-68-3; (E)-THPOCH2C- (CH,)=CHBr, 1 17582-49-7; (E)-Me02CC(CH3)=CHBr, 40053-01-8; o-BrC,H4(CH2)2CH=CH2. 7 181 3-50-8; PdC12(PhCN)2, 14220-64-5; octylbenzene, 21 89-60-8; iodobenzene, 591-50-4; trioctylborane, 3248- 78-0; tricyclopentylborane, 23985-40-2; tricyclohexylborane, 1088-01 -3; butylbenzene, 104-5 1-8; 5-iodo-1,3-benzodioxole, 5876-51-7; I-bromo- naphthalene, 90-1 1-9; l-(4-bromophenyl)ethanone, 99-90-1; 3-bromo- benzaldehyde, 31 32-99-8; methyl 4-iodobenzoate, 619-44-3; 1-octene, 11 1-66-0; 2-methyl-l-propene, 115-1 1-7; methyl IO-undecenoate, 11 1- 8 1-9; 2-methoxy-l-octylbenzene, 20056-59-1; 3,4-(methylenedioxy)-l- octylbenzene, 109636- 18-2; 1 -(2-methylpropyl)naphthalene, 16727-9 1-6; 4-( 10-carbomethoxy)acetophenone, 1 17582-38-4; 4-( 10-cyanodecany1)- acetophenone, 1 17582-39-5; 4-(6,7-epoxy-6-methyIhexyl)acetophenone, 1 1 7582-40-8; 3-[5,5-(ethylenedioxy)hexyl]benzaldehyde, 117582-41-9; methyl 4-( 10-carbomethoxydecanyl)benzoate, 109636-19-3; methyl 4- methylbenzoate, 99-75-2; 7-(4-acetylphenyl)-2-methylheptane- 1,2-diol, 1 17582-42-0; (E)-1-phenyl- 1-decene, 6