陶瓷材料综合实验技术指导书编写.pdf

陶瓷材料综合实验技术指导书 西南交通大学材料学院金属系 陈松 王良辉 编 西南交通大学 2014 年 08 月 陶瓷材料综合实验是材料科学与工程专业无机非金属专业方向的 专业实验课。通过实验本课程的学习，使学生掌握无机非金属材料制 备的基本过程及一些应用技术，了解无机非金属材料制备技术的发展 状况。理解无机非金属材料制备技术在生产和使用中的重要地位，培 养学生运用新技术进行材料研究开发、制备的能力。本实验是材料科 学与工程专业教学中的重要实践环节，旨在培养学生对常见无机非金 属材料的了解和认识，学习陶瓷材料和无机胶凝材料的典型制备方 法，加深学生对陶瓷材料和无机胶凝材料制备技术发展趋势的了解， 同时培养学生对基本设备的操作能力和实验动手能力。 - 1 - 目录 第 1 章 陶瓷热压烧结实验·····································································3 第 1 节 铝粉末热压成型技术 ··················· ·······································6 第 2 节 SiC 增强 Al 基复合陶瓷的热压制备·········································8 第 3 节 Al O 陶瓷的热压制备·························································10 2 3 第 4 节 ZrO 增强Al O 基复合陶瓷的热压制备···································12 2 2 3 第 2 章 陶瓷常规烧结实验····································································14 第 1 节 添加烧结助剂的功能陶瓷预烧工艺实验···································16 第 2 节 水溶液固相工艺制备陶瓷·····················································24 第 3 节 日用长石质瓷坯料配方设计··················································29 第 3 章 无机胶凝材料综合实验······························································37 第 1 节 水泥物理化学基本性质实验（验证性实验）·····························37 第 2 节 砌筑砂浆配合比设计···························································47 第 3 节 外加剂对水泥初凝时间的影响···············································54 第 4 节 外加剂对砂浆膨胀性能的影响·············································58 第 5 节 普通混凝土配合比设计························································61 参考文献··························································································73