磁悬浮天平吸附应用.ppt

MANOMETRIC全自动多样品高压气体吸附仪 Multi-sample high pressure volumetricsorption analyzer for application relevant characterization of sorbent materials Application Field: Material development Process development Chemical engineering Applications: Adsorbent Catalyst manufacturer Adsorption research Separation Gas storage process engineering MANOMETRIC全自动多样品高压气体吸附仪 Magnetic Suspension Balancefor high resolution weighing 0.001ug NANOMSB 纳克精度磁悬浮天平 Hanging sample version for highest P moderate T applications mSample 200 mg 1000 mg Dm 0.01 mg 0.1 mg Small volume / inner diameter - highest pressures possible ( 1000 bar) NANOMSB 纳克精度磁悬浮天平 Toploading version for high T high P TGA application mSample 200 mg 500 mg Dm 0.01 mg 0.1 mg Reduced convection - improved balance stability NANOMSB 纳克精度磁悬浮天平 High resolution Magnetic Suspension Balancefor measurements with small samples Application Field Material development Catalysis Applications: Adsorption research with rare new materials Gas storage research at highest pressures High P TGA measurements with rare materials/catalysis NANOMSB 纳克精度磁悬浮天平 MSB Working Principle – Video of Sample Area Balance 16.158 309 g Electromagnet Permanent Magnet Sensor Coil Load Decoupling Sample MSB Working Principle – Video of Load Decoupling Balance 16.158 309 g Electromagnet Permanent Magnet Sensor Coil Load Decoupling Sample MSB Working Principle – Video of Magnets Balance 16.158 309 g Electromagnet Permanent Magnet Sensor Coil Load Decoupling Sample * * * * * * * * * * * * * * * * * * * * 混合气体共吸附以及腐蚀性气体吸附 磁悬浮天平高压吸附仪 全自动实验控制和数据采集软件系统 可扩展性 温度控制模块 压力控制模块 测量池模块 色谱、质谱和红外连接 程序升温脱附TPD-MS，热脱附谱TDS 温度控制模块扩展 液氮等冷媒(77 K) 连续低温设备+恒温油浴 (120 K – 480 K) 电加热320 K – 780 K 应用：程序升温脱附 TPD 全自动气体引入和压力控制系统 全自动控制 vac – 15MPa, 35MPa, 70MPa 触摸屏交互式设计 实时显示工况 安全保护 H2 CH4 全自动气体引入和压力控制系统结构图 定制的较复杂全自动气体引入和压力控制系统 较复杂的整套磁悬浮天平重量法吸附分析系统 可视化测量池 P: 最高35MPa T: 最高200 C 可外加观察手段 - 摄像机、照相机 - 小型拉曼光谱 气氛敏感样品测量池 无水无氧 惰性环境 固定床测量池 模