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Identification of Urethane Linkage, Soft Segment （识别聚氨酯链接,软段）.pdf

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Identification of Urethane Linkage, Soft Segment （识别聚氨酯链接,软段）

World Applied Sciences Journal 26 (Natural Resources Research and Development in Sulawesi Indonesia): 50-54, 2013 ISSN 1818-4952 © IDOSI Publications, 2013 DOI: 10.5829/idosi.wasj.2013.26.nrrdsi.26009 Identification of Urethane Linkage, Soft Segment Polyol and Hard Segment Polyurea in Polyuretan from Palm Oil Based Polyol 1 1 1 1 2 La Ifa, Nurdjannah, Andi Aladin, Zakir Sabara and Kamaruzaman Jusoff 1Department of Chemical Engineering, Faculty of Industrial Technology, Jalan Urip Sumoharjo Km 05 Makassar, Universitas Muslim Indonesia, South Sulawesi, Indonesia 2Department of Forest Production, Faculty of Forestry, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor Darul Ehsan, Malaysia Submitted: Sep 24, 2013; Accepted: Nov 26, 2013; Published: Dec 20, 2013 Abstract: The objective of this paper is to identify the existence of urethane linkage, soft segment polyol and hard segment polyurea in polyurethane from palm oil-based polyol. The method used to produce this polyurethane is the one-shoot method. In this method, palm oil-based polyol and additives such as water, surfactant, catalyst and methylene chloride was mixed in a reactor, then toluene diisocyanate (TDI) was poured intothe reactor and stirred. Polyurethane produced was then poured into a cast and cured. The structure of polyuretan yielded was analysed by using Differensial Scanning Calorimeter to investigate soft segment dan hard segment polyurea. Fourier Transform Infra Red (FTIR) Spectroscopy was used to identify the existence of urethane linkage. Results indicated that the type o