TNAIA-枸杞及其制品中3中有机酸的测定-气相色谱法 .pdfVIP

ICS01.040.65

CCSB04

TB

T/NAIA-

3

2024-2024--

GB/T1.1-20201

3

1

3

2

()

GB/T6682

3

4

-

5

GB/T6682

5.1

5.1.1(HSO)

24

5.1.2(CHOH)

3

5.1.3(CHCl)

22

5.2

5.2.110%-10.0mL90mL

5.3

95%A

95%A

95%A

5.4

5.4.125mg/mL5.3

10mL25mg/mL

5.4.225mg/mL5.3

10mL25mg/mL

5.4.325mg/mL5.3

10mL25mg/mL

5.4.40.02mL0.04mL0.08mL0.20mL0.40mL0.80mL

310.0mL5.4.110%-

0.05mg/mL0.10mg/mL0.20mg/mL0.50mg/mL1.0mg/mL2.0mg/mL

22h50mL10mL10mL

2min

6

6.1FID

6.20.00001g0.01g

6.315000r/min

6.4

6.550mL

6.60.22μm

7

7.1

500g

7.2

0.5g50mL10mL10%-22

h10mL10mL5min0.22μm

7.3

7.3.1

a)HP-530m320μm×0.25μm),

b)

c)1μL

d)1.0mL/min

e)

f)2:1

g)260

h)300

i)1

1

/min(min)

0.0802

101802

1526010

7.4

8

1

CV

X1

m

óg/kg);

ómg/mL);

VómL);